By Klaus A. Hoffmann, Steve T. Chiang

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Reprinted with permission from [165] molecular interaction and the covalent interaction (Fig. 48). The “covalentcasting approach” is described as an approach to fix the supramolecularly ordered assemblies during the ordering process in their predetermined position. This leads to a highly cooperative ordering process, which ends up in the formation of highly organized molecular strands and ribbons. Extending this concept into disc-like aggregates [170] (Fig. 49) leads to discs and platelets, which can hold a photomodulative entity (azobenzene), which causes reversible aggregation and deaggregation phenomena based on the photoisomerization of the azobenzene moiety.

Fig. 19 Reversible attachment of a Cu(I)-catalyst to a solid support via triple hydrogen bonds, acting as a reversible catalyst for atom transfer radical polymerization (ATRP) Supramolecular Polymers and Networks 23 Fig. 20 Thymine-functionalized poly(styrene) for time-retarded drug release A similar strategy for the binding of flavines was presented by Rotello et al. [97–99] (Fig. 21). Here, Merrifield-resins bearing side-chain functionalized poly(styrenes) with 2,6-diamino-1,3,5-triazines were prepared and subjected to the binding of flavines via triple hydrogen bonds.

In the solid state, sheet-type structures are formed as studied by solid-state NMR spectroscopy, TEM- and thermal measurements. DSC methods clearly revealed the presence of two separate phases, whereas solid-state 13 C-MASNMR demonstrated the different chain mobility of the PEK- and PIB chains via relaxation measurements. The relevance of thymine/2,6-diaminotriazine interactions has been exploited by a variety of authors to effect a reversible, yet stable association of catalysts, nanoparticles and other functional molecules onto polymeric molecules.

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